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- W2092173276 abstract "The molecular complex [Ru(CO)3Cl2]2·SbCl3 has been prepared by reaction of antimony pentachloride and hydrogen chloride with ruthenium dodecacarbonyl in dichloromethane. Its molecular and crystal structure have been established by a single-crystal X-ray diffraction study. The structure consists of two crystallographically non-equivalent dimers Ru2(CO)6Cl4 with a double Ru−Cl−Ru bridge, each dimer interacting with SbCl3 units via Ru−Cl…Sb bonds. The coordination of the antimony trichloride fragment is discussed in terms of VSEPR (valence shell electron pair repulsion) on the assumption that the lone pair is playing a stereo-active role in the antimony environment. Crystallographic details: Space group: P21/c, Z=4, a=9.289(2) Å, b=11.986(2) Å, c=16.932 c=16.932(2) Å, β=100.31(2)°. Final agreement factor for data with I>3σ(I): R=0.05 for 1969 reflections." @default.
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- W2092173276 date "1981-07-01" @default.
- W2092173276 modified "2023-10-01" @default.
- W2092173276 title "Synthesis and structural characterization of the molecular complex [Ru(CO)3Cl2]2·SbCl3" @default.
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- W2092173276 doi "https://doi.org/10.1016/s0022-328x(81)80013-7" @default.
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