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• W2092309849 abstract "The reaction of 1-formyldipyrromethane (100 mM) in toluene at 115 °C containing DBU (10 mol equiv) and MgBr2 (3 mol equiv) in the presence of air affords the magnesium chelate Mg(II) porphine in 30−40% yield. The advantages of the new method include simplicity, high concentration, chromatography-free purification, gram-scale synthesis, and avoidance of the poorly soluble free base porphine. Mg(II) porphine exhibits good solubility in common organic solvents and is a valuable core scaffold for derivatization." @default.
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• W2092309849 date "2007-05-23" @default.
• W2092309849 modified "2023-10-02" @default.
• W2092309849 title "Direct Synthesis of Magnesium Porphine via 1-Formyldipyrromethane" @default.
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• W2092309849 doi "https://doi.org/10.1021/jo070532z" @default.
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