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• W2092330403 abstract "The metallocyclobutane complex Pt[C 3 H 2 (CN) 4 ]P(C 6 H 5 ) 3 ] 2 was prepared from the reaction between 1,1,2,2-tetracyanocyclopropane and Pt[P(C 6 H 5 ) 3 ] 4 . The crystal and molecular structure of this complex has been determined from three-dimensional X-ray diffraction data. The crystal has symmetry consistent with the space group P 1 ( C 1 i ) with two molecules of the complex in a unit cell of dimensions a 11.422(5), b 17.001(8), c 10.478(5) », α 107.27(2), β 110.72(2), γ 82.50(2)°. The structure was refined by least-squares techniques to a conventional R index of 0.035 based on 4553 reflections above background collected using a four-circle diffractometer. The structure determination shows that Pt[P(C 6 H 5 ) 3 ] 2 has inserted into the 1—2 carboncarbon of 1,1,2,2-tetracyanocyclopropane. Comparisons are made between the structural parameters of this complex and those of other metallocyclobutanes." @default.
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• W2092330403 date "1974-04-01" @default.
• W2092330403 modified "2023-10-02" @default.
• W2092330403 title "The structure of a metallocyclobutane complex, Pt[C3H2(CN)4][P(C6H5)3]2, the product of the reaction between 1,1,2,2-Tetracyanocyclopropane and Pt[P(C6H5)3]4" @default.
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• W2092330403 doi "https://doi.org/10.1016/s0022-328x(00)88254-6" @default.
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