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• W2092486171 abstract "The characterization of six silica-based reversed-phase liquid chromatographic columns was attempted by calculating characteristic interaction constants for the stationary phases based on linear solvation energy relationships. Four interaction properties of the stationary phase, m (the cavity formation/dispersive interaction strength), s (dipolarity/polarizability), b (hydrogen bond donating acidity) and a (hydrogen bond accepting basicity), are readily determined by multiple regression analyses of logarithmic capacity factors (k′) for a set of test solutes measured on it in an aqueous mobile phase of a given organic content versus the solute properties represented by the Van der Waals molar volume, Kamlet-Taft dipolarity/polarizability, π*, hydrogen bond accepting basicity, β, and hydrogen bond donating acidity, α. The magnitudes of the four constants vary with the type of bonded ligand and with brand in the case of stationary phases having the same ligand, while they generally decrease in the order m > b > a > s, regardless of the type of the organic modifier in the mobile phase for all six columns. Although the four interaction strength constants are not as general as the widely used Rohrschneider and McReynolds constants for GLC stationary phases, it is believed that they will be useful in choosing the best column for a given separation among a number of nominally equivalent columns and columns with different bonded functionality." @default.
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• W2092486171 date "1994-04-01" @default.
• W2092486171 modified "2023-09-24" @default.
• W2092486171 title "Characterization of some silica-based reversed-phase liquid chromatographic columns based on linear salvation energy relationships" @default.
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• W2092486171 doi "https://doi.org/10.1016/0021-9673(94)87002-0" @default.
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