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- W2092726847 abstract "Interlayer acetate anions in layered double hydroxyacetates of Ni2+ and Zn2+ have been exchanged by oxovanadates following three synthetic routes (at 60°C, under hydrothermal conditions and after preswelling with caprylate anions) and different pH; direct exchange at room temperature was not successful. Complete exchange was achieved under adequated conditions, and the precise nature of the interlayer anion depends on the pH during exchange: at low pH (4.5), the presence of α-VO3 chains, with anchoring (grafting) of the species to the hydroxide layers, is proposed. At higher pH (9.5) V2O74− species are present in the interlayer. Thermal decomposition of these vanadate-intercalated products leads to formation of orthorhombic Ni2+ and Zn2+ vanadates, together with NiO." @default.
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- W2092726847 date "2004-10-01" @default.
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- W2092726847 title "Intercalation of vanadate in Ni, Zn layered hydroxyacetates" @default.
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- W2092726847 doi "https://doi.org/10.1016/j.jssc.2004.05.055" @default.
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