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• W2092764103 abstract "Summary The analysis of lipid-phospholipid oxidation products is of primary importance. Although there are established HPLC and LC-MS techniques, it is shown here for the first time that the combination of matrix-assisted laser desorption and ionization time-of-flight (MALDI-TOF) mass spectrometry (MS) and TLC represents a sensitive, fast, and convenient alternative. A mixture of 1-palmitoyl-2-linoleoyl-sn-phosphatidylcholine (PLPC) and -ethanolamine (PLPE) was oxidized under the influence of atmospheric oxygen and characterized by direct positive ion MALDI-TOF MS as well as combined TLC-MALDI. It is shown that much more detailed information — particularly related to the oxidation products of PLPE that have so far been scarcely investigated — can be obtained by TLC-MALDI. However, it is also shown that further methodological improvements are necessary to make this method generally applicable to complex lipid mixtures." @default.
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• W2092764103 date "2011-06-01" @default.
• W2092764103 modified "2023-09-26" @default.
• W2092764103 title "A simple TLC-MALDI method to monitor oxidation products of phosphatidylcholines and -ethanolamines" @default.
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• W2092764103 doi "https://doi.org/10.1556/achrom.23.2011.2.13" @default.
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