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- W2092890504 abstract "An efficient method for the solid-supported synthesis of 5-N-alkylamino and 5-N-arylamino pyrazoles is described. This method is general and mild and utilizes readily accessible resin-immobilized beta-ketoamides 2 as starting materials for the preparation of 1. Resin-immobilized beta-ketoamide, aryl-, or alkylhydazine and Lawesson's reagent are suspended in a mixture of THF/Py and heated at 50-55 degrees C to give a resin-bound 5-aminopyrazole, that is liberated from the solid support by treatment with TFA." @default.
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- W2092890504 date "2005-05-17" @default.
- W2092890504 modified "2023-09-24" @default.
- W2092890504 title "Solid-Phase Synthesis of 5-Substituted Amino Pyrazoles" @default.
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- W2092890504 doi "https://doi.org/10.1021/cc049814s" @default.
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