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- W2092914456 abstract "Two ternary ligands consisting of two 2,2′:6′,2′′-terpyridines and one N4-quadridentate μ2,η2-bridging ligand were synthesized. The N4 bridge is 1,4-bis(2-pyridyl)phthalazine in ligand 1, and 3,6-bis(2-pyridyl)pyridazine in ligand 2. Two Co(II) dinuclear complexes [(1)Co2(μ-OH)]3+ and [(2)Co2(μ-OH)]3+, and one Ni(II) dinuclear complex [(1)Ni2(μ-Cl)]3+ were obtained. In the crystal structures of [(1)Co2(μ-OH)]3+ and [(1)Ni2(μ-Cl)]3+, two pyridine rings are twisted around the pyridine–phthalazine bonds to avoid steric repulsion between the hydrogen atoms. The pyridine rings also showed a significant tilt from the octahedral coordination plane, which causes the large positive shift of the first reduction potentials. Upon the addition of a proton, the cobalt dinuclear complexes can release one cobalt ion selectively, and the dinuclear complexes can be easily restored by the addition of a tertiary amine." @default.
- W2092914456 created "2016-06-24" @default.
- W2092914456 creator A5046381843 @default.
- W2092914456 creator A5073006246 @default.
- W2092914456 date "2013-01-01" @default.
- W2092914456 modified "2023-09-25" @default.
- W2092914456 title "New ternary ligands consisting of an N4 bridging ligand and two terpyridines, and their Co(ii) and Ni(ii) dinuclear complexes. Structure, redox properties, and reaction with acid" @default.
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- W2092914456 doi "https://doi.org/10.1039/c3dt33011g" @default.
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