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- W2092956330 abstract "N-Trichlorsilyl-pyrrol (I) wurde dargestellt und zusammen mit N-Trimethylsilyl-pyrrol (II) IR- und RAMAN–spektroskopiseh untersucht. Für Pyrrol, I, II und N-Silyl-pyrrol wurde eine Normalkoordinatenanalyse durchgeführt, aus der hervor-geht, daß keine charakteristische „SiN-Schwingung”︁ auftritt. Diese Schwingung ist vielmehr mit ν NC2 und δ(Ring) sowie γs SiC3 und γs SiCl3 gemischt und an mehreren Frequenzen zwischen ∼400 und ∼1100 cm−1 beteiligt. Die Ergebnisse werden mit quantenchemischen Berechnungen an Pyrrol und II verglichen. N-trichlorosilyl pyrrole (I) was prepared and, along with N-trimethylsilyl pyrrole (II), investigated by infrared and RAMAN spectroscopy. A normal coordinate analysis which was performed for pyrrole, I, II, and N-silyl pyrrole, suggests that no pure „SiN stretching frequency”︁ occurs. This mode is mixed with ν NC2 and δ(ring) as well as with vs SiC3 and vs SiCl3 and contributes to frequencies between ∼400 and ∼1100 cm−1. The results are compared with quantum chemical calculations for pyrrole and II." @default.
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- W2092956330 title "Schwingungsspektren und Normalkoordinatenanalyse von N-Silylpyrrolen C4H4NSiX3 (X = Cl, CH3, H)" @default.
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- W2092956330 doi "https://doi.org/10.1002/zaac.19713810207" @default.
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