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- W2093142418 abstract "Abstract Under specific conditions the reduction of the chlorophosphanes R(Me 2 NCH 2 2-C 6 H 4 )PCl or RPCl 2 [R=(Me 3 Si) 2 CH] with LiAlH 4 gives the diphosphanes {R(Me 2 NCH 2 2-C 6 H 4 )P} 2 ( 2 ) and RPHPHR ( 3 ), respectively, in moderate to good yields. Compound 2 may be obtained in higher yield from the reaction of {R(Me 2 NCH 2 2-C 6 H 4 )P}Li with PbI 2 . Compounds 2 and 3 have been characterised by multi-element NMR spectroscopy and the meso -diastereomers of both compounds have been characterised by X-ray crystallography. In the solid state both meso - 2 and meso - 3 adopt an antiperiplanar conformation." @default.
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- W2093142418 date "2002-08-01" @default.
- W2093142418 modified "2023-09-25" @default.
- W2093142418 title "Isolation and structural characterisation of two sterically crowded diphosphanes" @default.
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- W2093142418 doi "https://doi.org/10.1016/s0022-328x(02)01434-1" @default.
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