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• W2093144428 abstract "The quality of DOSY NMR data can be improved by careful pre-processing techniques. Baseline drift, peak shift, and phase shift commonly exist in real-world DOSY NMR data. These phenomena seriously hinder the data analysis and should be removed as much as possible. In this paper, a series of preprocessing operations are proposed so that the subsequent multivariate curve resolution can yield optimal results. First, the baseline is corrected according to a method by Golotvin and Williams. Next, frequency and phase shift are removed by a new combination of reference deconvolution (FIDDLE), and a method presented by Witjes et al. that can correct several spectra simultaneously. The corrected data are analysed by the combination of multivariate curve resolution with non-linear least square regression (MCR–NLR). The MCR–NLR method turns out to be more robust and leads to better resolution of the pure components than classic MCR." @default.
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• W2093144428 date "2004-08-01" @default.
• W2093144428 modified "2023-09-26" @default.
• W2093144428 title "Improved DOSY NMR data processing by data enhancement and combination of multivariate curve resolution with non-linear least square fitting" @default.
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• W2093144428 doi "https://doi.org/10.1016/j.jmr.2004.04.019" @default.
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