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- W2093233627 abstract "Production of chlorpyrifos via the phase-transfer-catalyzed reaction of O,O-diethylphosphorochloridothioate and the sodium salt of 3,5,6-trichloropyridin-2-ol was reinvestigated. The formation of sulfotep (the major byproduct) and the yield are influenced by the nature and concentration of the catalysts, temperature, stirring rate, and time of the reaction. The elucidation of the roles of different parameters influencing the end of the reaction have permitted us to perform the synthesis of chlorpyrifos on bench scale (0.3 M scale) under optimized conditionsusing the minimum amounts of catalysts (0.5 mol %)with 92% yield and 98.5% purity." @default.
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- W2093233627 date "2004-06-09" @default.
- W2093233627 modified "2023-10-17" @default.
- W2093233627 title "Reinvestigation of Phase-Transfer-Catalyzed Chlorpyrifos Synthesis" @default.
- W2093233627 cites W1582201760 @default.
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- W2093233627 doi "https://doi.org/10.1021/op049929k" @default.
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