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- W2093442988 abstract "The particle beam liquid chromatography/mass spectrometry (LC/MS) interface has been adapted to a double-focusing sector instrument of reversed geometry. Electron ionizaition (EI) mass spectra of single components injected through a loop or of mixtures separated via a reversed-phase LC column have been recorded. These are superimposable with EI mass spectra obtained via a direct-insertion probe. Sensitivity tests show that high picogram and low nanogram amounts of samples can be detected. Complete high-resolution mass spectra on standards (single components and mixtures) were recorded. Good accuracy (better than 5 mmu) was obtained in most cases on 5 μg samples. To illustrate the versatility of the system, mass-analysed ion kinetic energy scans and linked scans at constant B/E were obtained on the molecular ion of cholesterol (2.5 μg and 500 pg). Parameters relating to various parts of a commercial interface are briefly reported." @default.
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- W2093442988 date "1990-06-01" @default.
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- W2093442988 title "Particle beam liquid chromatography/mass spectrometry on a double-focusing high resolution mass spectrometer" @default.
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- W2093442988 doi "https://doi.org/10.1002/rcm.1290040606" @default.
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