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- W2093448674 abstract "Methyl amyloses have been prepared under various conditions and studied as model compounds for the determination of the substitution pattern in the polymer chain. After permethylation with iodomethane-d3 the glucosidic linkages were statistically cleaved by partial methanolysis or reductive cleavage. The distribution of substituents in the dimer-, trimer-, and tetramer fraction was determined by FAB-MS and MALDI-TOF-MS and compared with that calculated from the monomer composition. While a homogeneous methylation in water gave the expected random distribution, a reaction in Me2SO solution with sodium hydroxide and iodomethane yielded a methyl amylose with a surprising bimodal substitution pattern. A third example indicates a ds gradient in the sample as a result of topochemical reaction control." @default.
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- W2093448674 date "1996-09-01" @default.
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- W2093448674 title "Model studies on methyl amyloses: correlation between reaction conditions and primary structure" @default.
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- W2093448674 doi "https://doi.org/10.1016/0008-6215(96)00141-3" @default.
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