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• W2093462425 abstract "Structural relaxation in a temperature range from 32 to 62° K glass transition has been investigated, for the first time, for a nearly monodisperse polystyrene using a differential scanning calorimeter and a thermal mechanical analyzer. Low temperature anneals in the vicinity of 320 K stabilize the glassy structure and lead to volume contraction. Upon heating, the annealed samples show an excess endothermic peak and exhibit a gradual expansion associated with structural recovery above the annealing temperature. Significantly, the samples recover the initial heat content and volume without reheating through the glass transition temperature. This sub-Tg structural relaxation behavior is in many respects distinct from that commonly observed near the glass transition. Kinetics of relaxation processes are also discussed." @default.
• W2093462425 created "2016-06-24" @default.
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• W2093462425 date "1981-10-01" @default.
• W2093462425 modified "2023-10-16" @default.
• W2093462425 title "Sub-sub <i>T</i> <i>g</i> structural relaxation in glassy polymers" @default.
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• W2093462425 doi "https://doi.org/10.1063/1.329827" @default.
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