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- W2093559488 abstract "X-ray photoelectron (XPS) and Raman spectroscopic techniques have been used to study the influence of the annealing ambient (N2, Ar and H2) of nearly monodispersed Fe2O3 nanoparticles (mean size = 3.2 ± 1nm) on the growth of carbon nanotubes by microwave plasma chemical vapour deposition. XPS characterization of the catalytic templates reveals that a N2 ambient reduces sintering of the Fe2O3 nanoparticles and confirms that the chemical phase involved in the nucleation of nanotubes is the metal state Fe 0 . Multi-excitation wavelength Raman spectroscopy (514, 574, 633 and 785nm) reveals that the single-walled carbon nanotubes (SWCNTs) grown from N2-annealed catalyst nanoparticles range between 0.8 and 1.1nm while SWCNTs grown from Ar-annealed catalyst nanoparticles exhibit a broader diameter distribution in the range 0.8‐1.8nm. The narrowness in the distribution of SWCNTs grown from the N2-annealed catalysts has been attributed to the enhanced stability of Fe2O3 nanoparticles in an N2 ambient. (Some figures in this article are in colour only in the electronic version)" @default.
- W2093559488 created "2016-06-24" @default.
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- W2093559488 date "2008-07-31" @default.
- W2093559488 modified "2023-09-30" @default.
- W2093559488 title "XPS and Raman characterization of single-walled carbon nanotubes grown from pretreated Fe<sub>2</sub>O<sub>3</sub>nanoparticles" @default.
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- W2093559488 doi "https://doi.org/10.1088/0022-3727/41/16/165306" @default.
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