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- W2093576678 abstract "Dark-red, transparent crystals of potassium imido nitrido polytungstate(VI) (K14W6N16NH) were obtained by the reaction of tungsten powder with an excess of KNH2 in autoclaves at 600 °C for 6 days. The structure of this compound was determined from X-ray single-crystal data: space group, Pbcm; Z = 4, a = 9.738(3) Å, b = 12.527(4) Å, c = 24.04(1) Å; RRw = 0.0440.053 with N(Fo2) ⩾ 3σ(Fo2) = 1784, Nvar = 134. K14W6N16NH contains corner-sharing nitrogen tetrahedra around tungsten — [WN2N22] — which are linked together in six-membered rings in boat form. These rings are connected to each other in para-positions via imide groups — NH2− — to waved ropes which run along the b axis." @default.
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- W2093576678 date "1994-04-01" @default.
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- W2093576678 title "Synthesis and crystal structure of the potassium imido nitrido polytungstate(VI) K14W6N16NH" @default.
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- W2093576678 doi "https://doi.org/10.1016/0925-8388(94)90005-1" @default.
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