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• W2093657295 abstract "Fresh silica gels prepared by the sol–gel route with acid catalysis display typical alterations of the X-ray diffraction (XRD) pattern, in comparison with vitreous (v) silica. A positive shift of the first peak at k1 is noticed, which also shows excess broadening. The changes can be accounted for by the alteration of the intermediate-range order (IRO) in gels, in comparison with v-SiO2. Thermal annealing causes a gradual decrease in the shift and broadening of the first peak, suggesting that the evolution of the vitrification can be followed on the basis of XRD data. Two types of IRO alteration were modelled, which account quantitatively for the experimental observations using a phenomenological disorder parameter b. The evolution of the b values with annealing temperature reveals well-defined stages in the vitrification process." @default.
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• W2093657295 date "1997-06-01" @default.
• W2093657295 modified "2023-10-18" @default.
• W2093657295 title "Intermediate-Range Order in Silica Gels" @default.
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• W2093657295 doi "https://doi.org/10.1002/1521-396x(199706)161:2<317::aid-pssa317>3.0.co;2-x" @default.
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