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- W2093672890 abstract "Proton-coupled carbon-13 NMR spectra have been studied by a technique which involves Fourier transformation of spin echo modulation. When the protons are strongly coupled, the “proton flip” version of this experiment generates a new form of carbon-13 spectrum which is quite distinct from the multiplet structure of the conventional NMR spectrum. The transition frequencies and intensities are exactly symmetrical about the center frequency and some lines have negative intensities. Experimental spectra from the C2 site in pyridine are presented and analyzed by means of an iterative program derived from LAOCOON 111. The resulting proton-carbon coupling constants are in excellent agreement with those obtained by analysis of the conventional spectrum. The new program may also be used to calculate the echo modulation in strongly coupled homonuclear spin systems, and the echo modulation induced in heteronuclear systems by strongly coupled nonresonant spins." @default.
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- W2093672890 date "1977-10-01" @default.
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- W2093672890 title "Proton-coupled carbon-13 J spectra in the presence of strong coupling. II" @default.
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- W2093672890 doi "https://doi.org/10.1016/0022-2364(77)90252-9" @default.
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