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- W2093767854 abstract "The reaction of [Os3(CO)10(μ-dppm)] (1) with tBu2PH in refluxing diglyme results in the electron-deficient metal cluster complex [Os3(CO)5(μ3-H)(μ-PtBu2)2(μ-dppm)] (2) (dppm = Ph2PCH2PPh2) in good yields. The molecular structure of 2 has been established by a single crystal X-ray structure analysis. In contrast to the known homologue [Ru3(μ-CO)(CO)4(μ3-H)(μ-H)(μ-PtBu2)2(μ-dppm)] (3), no bridging carbonyl ligand was found in 2. The electronically unsaturated cluster 2 does not react with carbon monoxide under elevated pressure, therefore 2 seems to be coordinatively saturated by reason of the high steric demands of the phosphido ligands." @default.
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- W2093767854 date "1996-11-01" @default.
- W2093767854 modified "2023-09-27" @default.
- W2093767854 title "Synthesis and X-ray crystal structure of the electron-deficient metal carbonyl cluster [Os3(CO)5(μ3-H)(μ-H)(μ-PtBu2)2(μ-Ph2PCH2PPh2)]" @default.
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- W2093767854 doi "https://doi.org/10.1016/s0022-328x(96)06542-4" @default.
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