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- W2094134421 abstract "The molecular and crystal structure of (tricyclohexylphosphine)methylnickel(II) 2,4-pentanedionate has been determined by conventional Patterson and Fourier synthesis and refined anisotropically to a final R value of 0.08, including hydrogen atoms. Coordination about the nickel atom is square-planar with the angles subtended at the nickel being: O(1)NiO(2) = 93°; O(1)NiC(19) = 84°; C(19)NiP = 93°; PNiO(2) = 90°. The NiC(19) σ-bond length is 1.94(1) Å. The cyclohexyl rings are all in the chair conformation having an average CC distance of 1.53 Å and are bonded equatorially to the phosphorus in a tetrahedral arrangement with the average PC distance being 1.861 Å. The pentanedione ligand is planar within experimental error. Molecules of the title compound pack as discrete units in the crystal with no non-hydrogen intermolecular distance being less than 3.6 Å." @default.
- W2094134421 created "2016-06-24" @default.
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- W2094134421 date "1972-08-01" @default.
- W2094134421 modified "2023-10-03" @default.
- W2094134421 title "The molecular and crystal, structure of (tricyclohexylphosphine)methylnickel(II) 2,4-pentanedionate; A squareplanar complex containing a σ-nickel—carbon bond" @default.
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- W2094134421 doi "https://doi.org/10.1016/s0022-328x(00)81844-6" @default.
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