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• W2094331394 abstract "Star-shaped poly(ε-caprolactone) (PCL) with a fullerene (C60) core, C60[N(CH2)12OPCLOH]x, was successfully synthesized by reaction of azide-terminated PCL with C60. Both the experimental conditions and the stoichiometry were optimized, such that an average of six PCL chains was grafted per fullerene core. The molecular weight of the polyester chains directly controlled the length of the arms of the star-shaped polymers. Singlet oxygen was generated on irradiation of the C60[N(CH2)12OPCLOH]x nanohybrids. These C60[N(CH2)12OPCLOH]x nanohybrids were then processed in two kinds of nanomaterials. First, they were encapsulated within the core of micelles formed by biocompatible amphiphilic block copolymers. In water, the particle size distribution of these nanoparticles was narrow, and their diameter was in the range of 100 to 200 nm. Second, C60-containing micro-/nanosized polymer fibers were prepared, for the first time, by electrospinning. The average diameter of the fibers was varied by tuning the PCL/C60[N(CH2)12OPCLOH]x weight ratio. Grafting of polyester chains onto C60 is thus a suitable strategy for producing easily processable C60 and attractive building blocks for incorporation of C60 in nanomaterials." @default.
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• W2094331394 date "2006-09-09" @default.
• W2094331394 modified "2023-10-14" @default.
• W2094331394 title "New Nanostructured Materials Based on Fullerene and Biodegradable Polyesters" @default.
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• W2094331394 doi "https://doi.org/10.1021/cm060796m" @default.
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