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- W2094392718 abstract "Die Massenspektren von sechs NiII-Chelaten mit gleicher Ligandenperipherie aber unterschiedlichen Donoratomkombinationen (Atomsequenz der Liganden C(X)NHC(Y); X, Y = O, S, Se, NH; siehe Formelbild (1)) werden diskutiert. Die Fragmentierung der (Thio)Benzoyl-(thio,seleno)harnstoffkomplexe wird durch die Abgabe von S bzw. Se eingeleitet. Charakteristisch für die Fragmentierungsmuster aller Chelate ist die Abgabe kleiner neutraler Moleküle. Das NiII-Chelat mit einer NiS2Se2-Koordinationssphäre ist thermisch instabil; im Massenspektrum wird kein Molekülion beobachtet. Die Prozentsummen der Molekülionen der Chelate mit NiO4-, NiO2S2-, NiO2Se2-, NiN2S2- und NiS4-Koordination korrelieren mit der Komplexstabilität. Mass Spectrometric Fragmentation of NiII Chelates with O-, N-, S-, Se-Donor Atoms The mass spectra of 6NiII chelates having the same substituents but different donor atoms (sequence of ligand atoms C(X)NHC(Y); X, Y = O, S, Se, NH; see formula (1)) are discussed. The fragmentation pattern of the (thio)benzoyl(thio, seleno)ureas are characterized by the abstraction of S or Se atoms. The appearence of small neutral molecules seems to be typical for the fragmentation of all complexes. The mass spectrum of the NiII chelate having a NiS2Se2 coordination sphere shows no molecular ion peak. The contents of molecular ions in the total ion stream correlates with the stability of the complexes." @default.
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- W2094392718 date "1984-07-01" @default.
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- W2094392718 title "Die massenspektrometrische Fragmentierung von NiII-Chelaten mit O-, N-, S-, Se-Donoratomen" @default.
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- W2094392718 doi "https://doi.org/10.1002/zaac.19845140727" @default.
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