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- W2094592904 abstract "Abstract Methyl ester acetate derivatives of rat bile acids were analysed by a combined technique of solventless glass capillary gas chromatography and electron impact and ammonia chemical ionization mass spectrometry. Glass capillary columns ensure an excellent separating efficiency and effectiveness in detailed studies of many kinds of bile acid components. We found that the ammonia chemical ionization mass spectrometry gave (M + NH 4 ) + ions for all the methyl ester acetate derivatives of bile acids, and that these ions had intensities equal, or almost equal, to that of the base peak. This indicates that the technique is useful for the identification of unknown components, especially at trace levels. The results of electron impact and ammonia chemical ionization mass spectrometry of the major compound and the product obtained by catalytic hydrogenation of the compound indicated that this bile acid was a derivative of Δβ-muricholic acid having a double bond in the side-chain. We also found that most components had one double bond in their side-chain." @default.
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- W2094592904 date "1982-04-01" @default.
- W2094592904 modified "2023-09-26" @default.
- W2094592904 title "Characterization of bile acid methyl ester acetate derivatives of rat bile using solventless glass capillary gas chromatography and electron impact and ammonia chemical ionization mass spectrometry" @default.
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- W2094592904 doi "https://doi.org/10.1016/s0021-9673(00)82015-4" @default.
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