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• W2094724531 abstract "It has been predicted that the insulating properties of monodomain fatty acid Langmuir-Blodgett films should be much better than those fabricated by conventional techniques. Annealing of the monolayer on the water surface is a method which can in principle lead to oriented monolayers, and which has already been demonstrated to achieve modest reductions in disclination density in floating monolayers of 22-tricosenoic acid. In the present paper a previous report is extended by investigating the kinetics of disclination recombination in the same system, and determining how the rate constant correlates with annealing conditions. The phase behaviour of the system was found to be very similar to that of docosanoic acid, with superliquid, close-packed solid and L2′ phases in addition to the better-known liquid-condensed and solid phases. The kinetics in the liquid-condensed phase were found to be first order. This is to be expected if the molecules are tilted away from the substrate normal, so that disclinations are connected in pairs by twin boundaries. No significant correlation of the recombination rate with temperature or pressure was observed. Its functional dependence on the initial disclination density was consistent with a square root dependence, which is the expected law of variation of the inverse twin boundary length. There was a strong, essentially inverse, correlation with the period between sampling of the disclination density. It is concluded, and has been separately checked, that most of the recombination takes place during the sampling process, while the monolayer is being compressed for deposition onto a substrate and subsequently re-expanded, rather than while floating undisturbed, as was previously assumed." @default.
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• W2094724531 date "1989-11-01" @default.
• W2094724531 modified "2023-10-18" @default.
• W2094724531 title "Disclination recombination kinetics in water-surface monolayers of 22-tricosenoic acid" @default.
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• W2094724531 doi "https://doi.org/10.1016/0040-6090(89)90289-7" @default.
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