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- W2094785787 abstract "Abstract In the present work, the reliability of the responses obtained using an experimental TPD-MS system with the actual chemical process occurring at the reactor is investigated. The TPD-MS device operates in a flow of helium at normal pressure. The probable existence of fractioning phenomena was studied by comparing the responses of our system to instantaneous pulses of CO 2 and H 2 . In accordance with the results of our study, the analysis of evolved gases is not significantly disturbed by fractioning. In order to study the distortions induced by the system on the trace recorded at the MS for each of the gases analysed, the stimulus-response technique has been used. Instantaneous pulses of CO 2 were used as probe signals. Analysis of the responses of our TPD-MS system to the CO 2 pulses has been carried out by means of the so-called dispersed flow model. The dispersion moduli of the system were determined under different experimental conditions, which allowed optimization of the working conditions in order to achieve minimum distortion on the signals. The significance of perturbations induced by the system in a real TPD experiment was discussed by application of the principle of additivity of variances to the trace corresponding to the decomposition of MgCO 3 ." @default.
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- W2094785787 date "1986-02-01" @default.
- W2094785787 modified "2023-09-27" @default.
- W2094785787 title "Characterization of an experimental TPD-MS system. Reliability problems" @default.
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- W2094785787 doi "https://doi.org/10.1016/0040-6031(86)87102-7" @default.
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