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• W2094920300 abstract "Oxygen engineering techniques performed under adequate controlled atmosphere show that the CaMnO3−CaMnO2 topotactic reduction−oxidation process proceeds via oxygen diffusion while the cationic sublattice remains almost unaltered. Extra superlattice reflections in selected area electron diffraction patterns indicate doubling of the CaMnO2 rock-salt cell along the cubic directions of a distorted rhombohedral cell originated by ordering of Ca2+ and Mn2+ ions distributed in nanoclusters into a NaCl-type matrix, as evidenced by dark field electron microscope images. The local nature of the information provided by the transmission electron microscopy techniques used to characterize the rock-salt type Ca1−xMnxO2 solid solution clearly hints at the existence of subtle extra ordering in other upper oxides of the Ca−Mn−O system. The combination of local characterization techniques like electron microscopy with more average ones like powder X-ray and neutron diffraction allows a very complete characterization of the system." @default.
• W2094920300 created "2016-06-24" @default.
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• W2094920300 date "2009-05-29" @default.
• W2094920300 modified "2023-10-17" @default.
• W2094920300 title "Ordered Rock-Salt Related Nanoclusters in CaMnO₂" @default.
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• W2094920300 doi "https://doi.org/10.1021/ja901963m" @default.
• W2094920300 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/19480446" @default.
• W2094920300 hasPublicationYear "2009" @default.
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