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• W2094931247 startingPage "1285" @default.
• W2094931247 abstract "The reaction mechanism of elemental fluorine with the carbon material prepared by the pyrolysis of a fluorine–graphite intercalation compound (fluorine–GIC; CxF) has been discussed in detail. In spite of its large graphene sheets with the graphite-like stacking order, the pyrocarbon prepared from stage-1 C2.5F (ex-C2.5F pyrocarbon) exhibits a remarkably high reactivity against elemental fluorine even at room temperature which is comparable to that of carbon black. The small crystallite size along the c-axis of this pyrocarbon facilitates the expansion of every interlayer space and the formation of CF bonds on both sides of the carbon sheets at the early stage of the fluorination reaction. Ex-C2.5F pyrocarbons after the fluorination at 373 and 473 K are typical stage-1 CxF with semiionic CF bonds while those fluorinated at 573, 673 and 773 K are poly(carbon monofluoride) ((CF)n) with covalent CF bonds. The (CF)n with fairly high crystallinity along the c-axis is obtained by the fluorination of ex-C2.5F pyrocarbon above 673 K." @default.
• W2094931247 created "2016-06-24" @default.
• W2094931247 creator A5019328893 @default.
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• W2094931247 date "2003-09-01" @default.
• W2094931247 modified "2023-09-23" @default.
• W2094931247 title "Refluorination of pyrocarbon prepared from fluorine–GIC" @default.
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• W2094931247 doi "https://doi.org/10.1016/s1293-2558(03)00184-5" @default.
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