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- W2094932195 abstract "A series of new Ru(II) arene phosphine complexes derived from Binap have been prepared. Specifically, reaction of Ru(OAc)(2)(Binap) with 3,5-(CF(3))(2)C(6)H(3))(4)B (BArF).H(OEt(2))(2), is shown to afford new mono- and dinuclear Ru(II) hydroxyphosphine pi-arene complexes via a series of P-C bond cleavage reactions. The dinuclear Ru(II) pi-arene complexes contain bridging P(O)(OH)(2) ligands. Crystal structures of five new complexes are reported and suggest an eta(4)-arene rather than an eta(6)-arene coordination mode. However, in solution, their (13)C NMR data are more consistent with a strongly distorted eta(6)-coordination mode. PGSE (1)H and (19)F diffusion measurements on the dinuclear complexes suggest hydrogen bonding of the triflate anion and ion-pairing of the BArF(-) anion." @default.
- W2094932195 created "2016-06-24" @default.
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- W2094932195 date "2004-02-20" @default.
- W2094932195 modified "2023-09-24" @default.
- W2094932195 title "X-ray Diffraction and NMR Studies on a Series of Binap-Based Ru(II) Hydroxyphosphine π-Arene Complexes" @default.
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- W2094932195 doi "https://doi.org/10.1021/ic0352147" @default.
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