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• W2094955897 abstract "Abstract Nanoparticles of Ni 1− x Zn x O and Ni 1− x Zn x O/ZnO, which can be good candidates for selective gas sensors, were successfully obtained via a two-step synthetic route, in which the nickel zinc malonate precursor was first synthesized by co-precipitation from an aqueous solution, followed by pyrolysis in air at a relatively low temperature (~500 °C). The precursor was characterized by ICP-AES, FTIR and TG and the results indicate the molecular structure of the precursor to be compatible with Ni 1− x Zn x (OOCCH 2 COO)·2H 2 O. The decomposition product, characterized using various techniques (FTIR, XRD, ToF-SIMS, SEM, TEM and XPS), was established to be a doped nickel oxide (Ni 1− x Zn x O for 0.01≤ x ≤0.1) and a composite material (Ni 1− x Zn x O/ZnO for 0.2≤ x ≤0.5). To elucidate the form in which the Zn is present in the NiO structure, three analytical techniques were employed: ToF-SIMS, XRD and XPS. While ToF SIMS provided a direct evidence of the presence of Zn in the NiO crystal structure, XRD showed that Zn actually substitutes Ni in the structure and XPS is a bit more specific by indicating that the Zn is present in the form of Zn 2+ ions." @default.
• W2094955897 created "2016-06-24" @default.
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• W2094955897 date "2015-10-01" @default.
• W2094955897 modified "2023-09-23" @default.
• W2094955897 title "Coprecipitation of nickel zinc malonate: A facile and reproducible synthesis route for Ni1−Zn O nanoparticles and Ni1−Zn O/ZnO nanocomposites via pyrolysis" @default.
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• W2094955897 doi "https://doi.org/10.1016/j.jssc.2015.07.040" @default.
• W2094955897 hasPublicationYear "2015" @default.
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