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- W2094994819 abstract "The reaction between Ru3{μ3-PPhCH2PPh(C6H4)}(CO)9 (2) and HC2Ph resulted in insertion of a diene formed by coupling of the alkyne into an Ru–P(phosphido) bond to give a PPh(C6H4)CH2PPh(C4H2Ph2) ligand. Thermolysis regenerated the original phosphido–phosphine ligand and the alkyne dimer, which was coordinated in the usual 2η1:η4-mode. Similar metallacyclopentadiene complexes were obtained from 2 and HC2CO2Me, from Ru3{μ3-RC2(CO2Me)}(μ-dppm)(μ-CO)(CO)7 and C2Ph2 [R=CO2Me, H (2 isomers)], and from [Ru3(μ3-PPhCH2PPh2)(CO)9]− and C2Ph2, followed by protonation. X-ray structures are reported for the complexes Ru3{μ3-C2Ph2C2(CO2Me)2}(μ-dppm)(CO)6 (5) and two isomers of Ru3{μ3-C2Ph2 CHC(CO2Me)}(μ-dppm)(CO)6 (8a and 8b), Ru3{μ3-PPh(C6H4)CH2PPh(C4H2Ph2)}(μ-CO)(CO)6 (9) and Ru3(μ-H)(μ3-PPhCH2PPh2)(μ-C4Ph4)(CO)6 (12). In 5, 8a and 8b, one of the ester CO groups is bonded to an Ru atom also coordinated to phosphorus.Download : Download full-size imageDownload : Download full-size image" @default.
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- W2094994819 date "1998-02-01" @default.
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- W2094994819 title "Further observations on the dimerisation of alkynes on triruthenium clusters" @default.
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- W2094994819 doi "https://doi.org/10.1016/s0022-328x(97)00492-0" @default.
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