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- W2095151104 abstract "Abstract From an EtOH/H 2 O solution, 0.3 M each of Ni 2+ and cyclic triamine tacn ( 2 ; tacn=1,4,7‐triazacyclononane), after 10 min refluxing and cooling at room temperature, copious and comparable amounts of blue crystals (containing the complex [Ni(tacn)(H 2 O) 3 ] 2+ ) and pink crystals (containing in the same cell both [Ni(H 2 O) 6 ] 2+ and [Ni(tacn) 2 ] 2+ ) precipitated. This unusual behaviour is ascribed to the fact that at the refluxing temperature the three species are present at the equilibrium in similar concentrations, which are frozen on cooling, due to the inertness of the macrocyclic complexes [Ni(tacn)(H 2 O) 3 ] 2+ and [Ni(tacn) 2 ] 2+ ." @default.
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- W2095151104 date "2014-08-26" @default.
- W2095151104 modified "2023-10-18" @default.
- W2095151104 title "The Disproportionation of [Ni(tacn)]<sup>2+</sup>in Ni<sup>2+</sup>and [Ni(tacn)<sub>2</sub>]<sup>2+</sup>Crystallographically Demonstrated (tacn=1,4,7-Triazacyclononane)" @default.
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- W2095151104 doi "https://doi.org/10.1002/chem.201403969" @default.
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