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- W2095304944 abstract "Stereoselective Synthesis of 3-Substituted Cyclobutanols and Products Derived Therefrom 3-Substituted cyclobutanones 2 are prepared by alkene/dichloroketene cycloadditions and subsequent dehalogenation. Reduction with LiAlH(OtBu)3 furnishes cis-cyclobutanols 3 in 95–100% selectivity. Mitsunobu inversion turned out to be the only practical method to get trans isomers 4 in high selectivity. A stereoselective cyclobutanol→bromocyclobutane conversion could be achieved only by a modified Mitsunobu reaction. Cross coupling between zinc derivatives of bromocyclobutanes 9 and aromatic bromides is not stereoselective." @default.
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- W2095304944 date "1993-12-01" @default.
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- W2095304944 title "Stereoselektive Synthese von 3‐substituierten Cyclobutanolen und Folgeprodukten" @default.
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- W2095304944 doi "https://doi.org/10.1002/cber.19931261228" @default.
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