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- W2095321101 abstract "2-Heterocyclic/acyclicamino/4'-acetamidophenoxy-3-(4-chlorophenyl)-3,4-dihydrobenzo-[ e ][1,3,2]oxazaphosphinine 2-sulfides (4a-j) were synthesized through a two steps process. In the first step, 2-chloro-3-(4-chlorophenyl)-3, 4-dihydrobenzo[ e ] [1,3,2]-oxazaphosphinine 2-sulfide (2) was prepared by the reaction of 2-[(4-chlorophenylamino)methyl]phenol (1) with thiophosphoryl chloride in the presence of triethylamine in dry toluene-tetrahydrofuran. In the second step, 2 was treated with various heterocyclic/acyclicamines/4'-acetamidophenol in presence of triethylamine-/ sodium hydride in toluene-tetrahydrofuran at 45-50°C . All the synthesized compounds (4a-j) were characterized by elemental analysis, IR, NMR( 1 H, 13 C and 31 P) and mass spectra and their biological activity was evaluated for antimicrobial activity." @default.
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- W2095321101 date "2008-01-01" @default.
- W2095321101 modified "2023-10-16" @default.
- W2095321101 title "Synthesis and Biological Activity of Some new 2-Heterocyclic/acyclic amino/4'-acetamidophenoxy-3-(4-chloro-phenyl)-3, 4-dihydrobenzo[e]- [1,3,2]oxazaphosphinine 2-sulfides" @default.
- W2095321101 cites W575693177 @default.
- W2095321101 doi "https://doi.org/10.1155/2008/415030" @default.
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