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- W2095508052 abstract "Abstract The reaction of a 1:2 molar ratio of Cp3Pr with diethyl malonate in n-hexane results in the formation of {CpPr[CH(COOC2H5)2] [μ-CH(COOC2H5)2]}2. X-ray analysis demonstrates that the complex is a dimer, the two praseodymium atoms are bridged by two oxygen atoms of two independent diethyl malonate ligands. The bridging ligands coordinate with the praseodymium atom in a tridentate mode. the other two diethyl malonate ligands coordinate with praseodymium in a bidenate mode. The complex crystallizes in the monoclinic system, space group P 2 1 a with unit cell constants a=9.675(4), b=18.134(3), c=12.795(3) A , β=92.53(3)° . Dc = 1.55 g cm−3. M r = 1048.65, V = 2243(2) A 3 , for Z = 2, μ = 22.01 cm −1 and F(000) = 1056 . The structure was solved by heavy atom methods ( Dirdif ) and full-matrix least-squares refinement to the final R = 0.040, Rw = 0.048." @default.
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- W2095508052 date "1996-10-01" @default.
- W2095508052 modified "2023-09-27" @default.
- W2095508052 title "Synthesis and structural investigation of {CpPr[CH(COOC2H5)2][μ-CH(COOC2H5)2]}2" @default.
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- W2095508052 doi "https://doi.org/10.1016/0022-328x(96)06415-7" @default.
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