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- W2095641384 abstract "Abstract Electro‐oxidation of Ce(III) to Ce(IV) in nitric acid media at different anode materials with high oxygen evolution overpotential was carried out. Ce(IV) nitrato complexes were adsorbed on a novel resin, based on porous silica beads with immobilized polystyrene/DVB copolymer, that was impregnated with tri‐n‐butyl phosphate (TBP). Under the studied conditions, Ce(IV) sorption increased with increasing nitric acid concentration (0.5–6 mol · dm−3). Oxidation of sorbent by adsorbed Ce(IV) species resulting in Ce(III) release to the solution was observed and thoroughly evaluated. In spite of problems with TBP leakage (12%), column separation of pure Ce(IV) from Y(III) and La(III) was achieved in 6 mol · dm−3 HNO3 at 288 K. Ce(IV) breakthrough capacity was 0.48 mol · kg−1‐TBP. Column regeneration with 0.1 mol · dm−3 nitric acid yielded Ce solution with purity higher than 99.99 wt.% with respect to La and Y impurities." @default.
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- W2095641384 date "2006-10-01" @default.
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- W2095641384 title "Separation of Electrochemically Generated Ce(IV) from Rare Earths(III) in Nitric Acid Media by TBP Impregnated Resin" @default.
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- W2095641384 doi "https://doi.org/10.1080/07366290600846182" @default.
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