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- W2095806836 abstract "Abstract A capillary electrophoresis‐inductively coupled plasma‐mass spectrometric (CE‐ICP‐MS) method for the speciation of six arsenic compounds, namely arsenite [As(III)], arsenate [As(V)], monomethylarsonic acid, dimethylarsinic acid, arsenobetaine and arsenocholine is described. The separation has been achieved on a 70 cm length×75 µm ID fused‐silica capillary. The electrophoretic buffer used was 15 m M Tris (pH 9.0) containing 15 m M sodium dodecyl sulfate (SDS), while the applied voltage was set at +22 kV. The arsenic species in biological tissues were extracted into 80% v/v methanol‐water mixture, put in a closed centrifuge tube and kept in a water bath, using microwaves at 80°C for 3 min. The extraction efficiencies of individual arsenic species added to the sample at 0.5 µg As/g level were between 96% and 107%, except for As(III), for which it was 89% and 77% for oyster and fish samples, respectively. The detection limits of the species studied were in the range 0.3–0.5 ng As/mL. The procedure has been applied for the speciation analysis of two reference materials, namely dogfish muscle tissue (NRCC DORM‐2) and oyster tissue (NIST SRM 1566a), and two real‐world samples." @default.
- W2095806836 created "2016-06-24" @default.
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- W2095806836 date "2005-04-01" @default.
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- W2095806836 title "Speciation of arsenic compounds in fish and oyster tissues by capillary electrophoresis-inductively coupled plasma-mass spectrometry" @default.
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- W2095806836 doi "https://doi.org/10.1002/elps.200410116" @default.
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