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• W2096077942 abstract "A series of novel bis[3,4,12,13,21,22,30,31-octa(dodecylthio)-2,3-naphthalocyaninato] rare earth(III) complexes M [ Nc ( SC 12 H 25 ) 8 ] 2 ( M = Nd , Eu , Gd , Tb , Y , Ho , Er ) have been prepared by tetramerization of 2,3-bis(dodecylthio)-6,7-dicyanonaphthalene with M ( acac ) 3 ·n H 2 O in the presence of 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) in refluxing n-octanol. These sandwich double-decker complexes were characterized by elemental analysis and various spectroscopic methods including UV-vis, near IR, IR, and mass spectroscopies. Their liquid crystal behavior was studied by polarized optical microscope (POM), differential scanning calorimeter (DSC), and X-ray diffraction. These alkylthio-substituted bis(2,3-naphthalocyaninato) rare earth complexes yield a hexagonal columnar liquid crystal whose stable temperature range is between 42 and 243°C. The stable temperature domain of the mesophase shows a trend to be dependent on the central rare earth ionic size. In contrast, the molecular packing of these complexes as revealed by X-ray diffraction was found to be almost independent of the ionic size of the central rare earth." @default.
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• W2096077942 date "2006-09-01" @default.
• W2096077942 modified "2023-09-24" @default.
• W2096077942 title "Synthesis and liquid crystal behavior of bis[3,4,12,13,21,22,30,31-octa(dodecylthio)-2,3-naphthalocyaninato] rare earth complexes" @default.
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• W2096077942 doi "https://doi.org/10.1142/s108842460600048x" @default.
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