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• W2096751706 abstract "Abstract Germanium(II) compounds featuring β‐diketiminate‐type ligands are attractive for applications as nanoparticle precursors, imaging agents, and components of electronic devices. In this work, we report the synthesis of β‐diketiminatogermanium(II) amides L′Ge(NHPh) [ 1 , L′ = {HC(CMeN–2,4,6‐Me 3 C 6 H 2 ) 2 } – ], L′Ge(4‐NHPy) ( 2 ), L′Ge(2‐NHPy) ( 3 ), and LGe(2‐NHPy) ( 4 ), L = {HC(CMeN–2,6‐ i Pr 2 C 6 H 3 ) 2 } – ], which were obtained by the reaction of a low‐valent organogermanium halide (L′GeCl or LGeCl) with a lithium salt of the respective aromatic amine (LiNHPh) or aminopyridine [Li(4‐NHPy) and Li(2‐NHPy)]. Compounds 1 – 4 were characterized with several techniques such as melting point, FTIR, 1 H and 13 C NMR spectroscopy, elemental analysis, X‐ray diffraction, and thermogravimetric analysis (TGA). Compounds 1 – 3 and 4 crystallized in the orthorhombic (space group Pnma ) and monoclinic (space group P 2 1 / c ) crystal systems, respectively. In all cases, the geometry around the central germanium atom was highly tetrahedrally distorted. According to TGA data, 1 – 4 do not sublime intact but rather exhibit thermal decomposition." @default.
• W2096751706 created "2016-06-24" @default.
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• W2096751706 date "2014-09-05" @default.
• W2096751706 modified "2023-10-10" @default.
• W2096751706 title "Monomeric Germanium(II) Amides Bearing β‐Diketiminato Ligands: Synthesis, Structural Characterization, and Thermal Properties" @default.
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• W2096751706 doi "https://doi.org/10.1002/ejic.201402594" @default.
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