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- W2097631549 abstract "Abstract The isotopically labelled C ‐terminal fragment of zervamicin, H‐Hyp 10 ‐[4,4‐ 2 H 2 ‐Gln]‐Aib‐Hyp‐Aib‐Pro‐Phl 16 , has been synthesized in solution by a Fmoc/ tert ‐butyl strategy in 28% overall yield. The Fmoc group was removed by reaction for 2 min with 0.1 M NaOH in dioxane/methanol/water, (30:9:1, v:v:v). The couplings of the sterically hindered Aib residues were achieved by means of either BOP/DMAP activation or Fmoc‐Aib‐Cl. Acid deprotection of the peptide was performed by reaction with 50% TFA in CH 2 Cl 2 for 30 min without significant cleavage of the acid‐labile Aib‐Pro and Aib‐Hyp peptide bonds." @default.
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- W2097631549 date "1997-01-01" @default.
- W2097631549 modified "2023-09-23" @default.
- W2097631549 title "Synthesis of the Isotopically LabelledC-Terminal Fragment of Zervamicin: An Approach to the Synthesis of Aib-Containing Peptides" @default.
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- W2097631549 doi "https://doi.org/10.1002/jlac.199719970109" @default.
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