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• W2097805972 abstract "• We coated Pt-15%Rh foil electrochemically with Hg. • The TG curve of Pt-15%Rh/Hg foil shows four distinct mass loss steps. • At the end of the first mass loss step only bulk Hg is removed. • In the second mass loss step only PtHg 4 , characterized by XRD, is decomposed. • In the third and in the fourth mass loss step the PtHg 2 and RhHg 2 are decomposed and Hg is removed from a solid solution of Pt-15%Rh(Hg). Thermogravimetry (TG), energy dispersive X-ray microanalysis (EDX), scanning electron microscopy (SEM), mapping surface and X-ray diffraction (XRD) were used for the study of solid-state reaction on Pt-15%Rh with electrodeposited mercury. The results suggest when heated the mercury film react with the Pt-15%Rh alloy to form intermetallics having different thermal stabilities indicated by three mass loss steps. The first mass loss step occurs between room temperature and 184 °C only the bulk Hg is removed and PtHg 4 , PtHg 2 and RhHg 2 were characterized by XRD. The second step, between 184 and 271 °C, was attributed to PtHg 4 decomposition with formation of PtHg 2 stabilized by RhHg 2 . The third step, between 271 and 340 °C, was attributed to decomposition of a solid-solution of PtHg 2 /RhHg 2 . The fourth step, between 340 and 600 °C, was ascribed to: (1) a thermal decomposition of PtHg 2 , formed by a PtHg eutectoid reaction (∼340 °C) on the surface and (2) Hg removal from a solid solution of Pt-15%Rh(Hg)." @default.
• W2097805972 created "2016-06-24" @default.
• W2097805972 creator A5042483021 @default.
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• W2097805972 date "2013-12-01" @default.
• W2097805972 modified "2023-10-03" @default.
• W2097805972 title "Thermal study of the solid-state reactions on Pt-15%Rh/Hg system" @default.
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• W2097805972 doi "https://doi.org/10.1016/j.tca.2013.09.021" @default.
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