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- W2098107967 abstract "A specially designed specimen holder employing a beryllium dome has been fabricated for collection of X-ray diffraction (XRD) data from highly reactive materials. The specimen holder has a robust O-ring type seal (<10 −9 Torr ) and no observed intensity artifacts in the 1° to 150° 2 θ range. The design also minimizes specimen displacement errors and allows for analysis of both powders and bulk specimens (i.e., pellets). The simple design makes for straightforward assembly of the holder within the confines of a glove box. XRD analysis of hygroscopic LaBr 3 powders collected with this holder are suitable for Rietveld structure refinement, yielding unit cell lattice parameters of a =7.9703(6) Å and c =4.5122(6) Å; cell volume=248.44(6) Å 3 ; R p =7.70%." @default.
- W2098107967 created "2016-06-24" @default.
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- W2098107967 date "2008-06-01" @default.
- W2098107967 modified "2023-10-12" @default.
- W2098107967 title "A beryllium dome specimen holder for XRD analysis of air sensitive materials" @default.
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- W2098107967 doi "https://doi.org/10.1154/1.2912452" @default.
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