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- W2098264472 abstract "4-tert-Butylcalix[4]arene (4tBC4A) is a versatile host capable of forming a variety of 1:1 and 2:1 inclusion compounds typically stabilized through van der Waals interactions. Preliminary studies in our group have demonstrated that inclusion of n-butylamine in 4tBC4A results in a series of pseudopolymorphic inclusion compounds, including a new 3:1 inclusion motif. Using a combination of SCXRD, TGA, solid state NMR, and PXRD, we now elaborate upon the relationship between these pseudopolymorphs. We also demonstrate that larger amines demonstrate a similar degree of pseudopolymorphism, allowing for the production of customized materials using self-assembly guided by competing weak forces. Finally, we comment on the structural implications of the relative dominance such forces in the formation of calixarene-based supramolecular frameworks." @default.
- W2098264472 created "2016-06-24" @default.
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- W2098264472 date "2006-11-06" @default.
- W2098264472 modified "2023-09-23" @default.
- W2098264472 title "Pseudopolymorphism of Aliphatic Amine/4-tert-Butylcalix[4]arene Inclusion Compounds: Supramolecular Stabilization as a Route to Polar Clusters and Layers" @default.
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- W2098264472 doi "https://doi.org/10.1002/chem.200600434" @default.
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