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- W2098865714 abstract "Charge transfer (CT) complexes of 4-(dimethylamino)pyridine (DMAP) with iodine as a typical σ-type acceptor and with typical π-type acceptor, 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ), have been synthesized and characterized. Octafluorotoluene (OFT), octafluoronaphthalene (OFN), perfluorophenanthrene (PFP), and 2,3,5,6-tetrafluoropyridine-4-carbonitrile (TFP) were also used as acceptors for interaction with DMAP. Properties of such CT complexes were investigated by UV/VIS and IR spectra, and elemental analyses of the isolated complexes. The systems DMAP-iodine and DMAP-DDQ are characterized by formation of triiodide ions (I 3 - ) and DDQ •- anion radicals, respectively, which is proposed to occur via initial formation of outer-sphere CT complexes. The systems (DMAP-OFT, DMAP-OFN, DMAP-PFP and DMAP-TFP) are characterized by the appearance of new UV/VIS spectral bands assigned as CT bands; they also furnished the corresponding solid complexes with the stoichiometric ratio 1:1. 1 H and 19 F NMR spectra were used on confirming the formation of the DMAP-PFP CT complexes. The formation constants ( K CT ) and molar absorption coefficients (ε CT ) of the latter complex were obtained." @default.
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- W2098865714 date "2006-01-01" @default.
- W2098865714 modified "2023-09-25" @default.
- W2098865714 title "Charge Transfer Molecular Complexes of 4-(Dimethylamino)pyridine with Some Conventional and Unconventional Acceptors Involving Fluoroarenes" @default.
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- W2098865714 doi "https://doi.org/10.1135/cccc20061359" @default.
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