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- W2098889090 abstract "Abstract The iron(II) clathrochelates with apical adamantyl substituents were synthesized by the direct template reaction on a metal ion matrix. The nucleophilic substitutions of reactive hexachloride precursors with adamantylthiolate anion afforded hexa- and octaadamantyl cage iron(II) complexes. Clathrochelates obtained have been characterized using elemental analysis, MALDI-TOF mass, IR, UV–Vis, 57 Fe Mossbauer and 1 H, 13 C NMR spectroscopies, and X-ray crystallography. Configurations intermediate between trigonal prismatic and trigonal antiprismatic have been deduced for the low-spin iron(II) ion coordination polyhedra of all clathrochelates obtained using 57 Fe Mossbauer parameters and confirmed by X-ray crystallography data. Two apical and up to six ribbed adamantyl substituents allow one to change the physical properties of clathrochelates synthesized in wide range. In particular, these substituents form second (hydrophobic) shell that opens up the possibility to membrane and cellular transport of the cage complexes." @default.
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- W2098889090 date "2007-04-01" @default.
- W2098889090 modified "2023-10-11" @default.
- W2098889090 title "Cage iron(II) complexes with apical and ribbed adamantyl substituents: The creation of second (hydrophobic) shell of an encapsulated metal ion" @default.
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- W2098889090 doi "https://doi.org/10.1016/j.ica.2006.08.036" @default.
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