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- W2099071749 abstract "The wavelength tunability and high intensity of a dedicated synchrotron X-ray source were extensively used in four-azimuth double-crystal diffraction experiments to study synthetic diamonds with (001) polished faces. These had major growth sectors of {001} and {111} type and some minor sectors of {110} and {113}. Many series of topographs (up to 80 per sample) in symmetric Bragg reflection geometry were recorded. Some of the common features frequently present in synthetic diamonds, namely metallic cylindrical inclusions as well as the growth sectors and growth sector boundaries, were the subject of this study. The presence of any source of strain in the crystal may seriously affect its performance in applications: mechanical (tools), optical (IR windows) or electronic (radiation detectors). X-Ray “pinhole” rocking curve measurements as well as detailed analysis of the topographic records yielded interesting new results concerning the state of the lattice in close proximity to each inclusion and inside growth sectors of the minor forms of {113} and {110} type. The axisymmetric strain field caused by the embedded body of each cylindrical inclusion was recorded as a symmetrically compressed lattice. The lattice parameter of the {113} growth sectors was found to be smaller (by 7 ppm) than that of the surrounding major growth sectors. More importantly, it is recorded and reported here for the first time that in addition to lattice parameter differences there exists significant lattice bending (radius R = 7.5 m) inside the minor sectors that is created by the compressive action of the surrounding major {001} and {111} growth sectors. Previous experiments have been unable to record this component of stress in synthetic diamonds either because of an inappropriate choice of diffraction geometry or because of incompleteness of the experimental procedures." @default.
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- W2099071749 date "1996-11-01" @default.
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- W2099071749 title "Synchrotron X-ray studies of strain in (100)-oriented high pressure-high temperature (HP-HT) synthetic diamonds" @default.
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- W2099071749 doi "https://doi.org/10.1016/0925-9635(96)00540-7" @default.
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