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• W2099255468 abstract "Abstract A novel mononuclear metal–organic compound, N-chloromethyl-1,4-diazabicyclo-[2.2.2]octonium trichloroaquomanganese (II), Mn(LCH 2 Cl) (H 2 O) Cl 3 ( 1 ) (L + CH2Cl = N-chloromethyl-1,4-diazabicyclo[2.2.2]octonium ion) was synthesized. Differential scanning calorimetry (DSC) measurement detected that this compound underwent a reversible phase transition at ca. 187.5 K with a hysteresis of 1.5 K width, The single crystal X-ray diffraction data suggested that the phase transition undergoes from a room temperature paraelectric phase with a space group of Pnma ( a  = 18.219(1) A, b  = 8.945(6) A, c  = 8.191(5) A, V  = 1334.9(2) A 3 and Z  = 4) to a low temperature paraelectric one with a space group of P2 1 /n ( a  = 8.117(2) A, b  = 17.956(5) A, c  = 8.923(2) A, β  = 91.819(3)°, V  = 1299.9(6) A 3 and Z  = 4), and symmetry breaking occurred with an Aizu notation of mmmF2/m. The ordering of twisting motions of dabco ring may drive the phase transition." @default.
• W2099255468 created "2016-06-24" @default.
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• W2099255468 date "2014-08-01" @default.
• W2099255468 modified "2023-09-23" @default.
• W2099255468 title "Temperature-induced reversible structural phase transition of N-chloromethyl-1,4-diazabicyclo[2.2.2]octonium trichloroaquo-manganese(II)" @default.
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• W2099255468 doi "https://doi.org/10.1016/j.molstruc.2014.05.041" @default.
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