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- W2099287750 abstract "A new laboratory x-ray absorption fine structure (XAFS) spectrometer specially designed for measurements of the absorption spectra of light elements is presented. The spectrometer consists of a newly developed rotating-anode x-ray source of portable size, a power supply of low-voltage and high-current type, a vacuum x-ray path, a Johann-type curved monochromator, a cell unit for high-temperature measurements, and a solid-state detector (SSD) system with a single-channel analyser. The SSD system can eliminate x-rays of other orders to give x-ray absorption data containing no noise due to high frequencies. A current control method is employed to suppress characteristic x-rays emitted from filament and target materials. The performance of the spectrometer was evaluated by x-ray absorption measurements on a copper foil at the Cu K-edge at room temperature and on powdered gibbsite and aluminosilicates at the Al K-edge. The results showed that the spectrometer is capable of obtaining good quality XAFS and x-ray absorption near-edge structure (XANES) spectra at Al and Cu K-edges within about 2 h. Thus, both XAFS and XANES studies will be possible with the spectrometer for a wide range of elements from sodium to lanthanides by use of suitable monochromator crystals." @default.
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- W2099287750 date "1992-03-01" @default.
- W2099287750 modified "2023-09-25" @default.
- W2099287750 title "Laboratory XAFS spectrometer for x-ray absorption spectra of light elements" @default.
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- W2099287750 doi "https://doi.org/10.1002/xrs.1300210209" @default.
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