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- W2100091836 abstract "The synthesis of a new series of alkanolamine esters is described. Esterification of 1,1′-iminodi-2-propanol with benzoyl chloride applying the Schotten-Baumann conditions afforded either the mono or diester according to the molecular ratio of the reactants but never the amide. With the more powerful acylating agent p-nitrobenzoyl chloride the diester-amide was always obtained even when equimolecular amounts of the reactants were used. Esterification of the N-methyl derivative of the amino alcohol with benzoyl chloride yielded in all cases the diester while esterification via the interaction of the dichloro analog of the amino alcohol and the appropriate silver salt invariably yielded the monoester even when excess of the silver salt was used. The synthesis of a new series of alkanolamine esters is described. Esterification of 1,1′-iminodi-2-propanol with benzoyl chloride applying the Schotten-Baumann conditions afforded either the mono or diester according to the molecular ratio of the reactants but never the amide. With the more powerful acylating agent p-nitrobenzoyl chloride the diester-amide was always obtained even when equimolecular amounts of the reactants were used. Esterification of the N-methyl derivative of the amino alcohol with benzoyl chloride yielded in all cases the diester while esterification via the interaction of the dichloro analog of the amino alcohol and the appropriate silver salt invariably yielded the monoester even when excess of the silver salt was used." @default.
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- W2100091836 date "1968-06-01" @default.
- W2100091836 modified "2023-09-26" @default.
- W2100091836 title "New Compounds: Certain Alkanolamine Esters Likely to Possess Anesthetic Activity" @default.
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- W2100091836 doi "https://doi.org/10.1002/jps.2600570645" @default.
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