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• W2100157834 abstract "4,5-Dineopentoxyphthalonitrile was prepared from catechol and neopentyl tosylate in three steps. Condensation of this substituted phthalonitrile with lithium metal in 1-pentanol led to 2,3,9,10,16,17,23,24-octaneopentoxyphthalocyanine. Lithiation in tetrahydrofuran gave the dilithium phthalocyanine which on methylation did not give the expected N -methylated product 29,31-dimethylphthalocyanine. The precipitate formed on methylation appeared to be the N + - CH 3 derivative in which one of the peripheral nitrogens was N -methylated. Methylation with 13 CH 3 I likely yielded an N + -methylated phthalocyanine having the requisite increased mass in its mass spectrum." @default.
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• W2100157834 date "2000-08-01" @default.
• W2100157834 modified "2023-09-27" @default.
• W2100157834 title "Towards <font>N</font>-alkylated phthalocyanines using 2,3,9,10,16,17,23,24-octaneopentoxyphthalocyanine" @default.
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• W2100157834 doi "https://doi.org/10.1002/1099-1409(200008)4:5<484::aid-jpp264>3.0.co;2-1" @default.
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